HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chlorobenzenesulfonyl chloride → 4-chloro-N-[5-chloro-2-(methylthio)phenyl]benzenesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chlorobenzenesulfonyl chloride | HCID 7398 | — |
| Reactant | 5-Chloro-2-(methylthio)aniline | HCID 2794577 | — |
| Product | 4-chloro-N-[5-chloro-2-(methylthio)phenyl]benzenesulfonamide | HCID 47419232 | 68% |
Reaction Steps
Following General Procedure B, the title compound (150 mg, 68%) was prepared from 5-Chloro-2-methylsulfanyl-phenylamine (110 mg, 0.64 mmol) and 4-Chloro-benzenesulfonyl chloride (134 mg, 0.64 mmol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09328067B2 |
| Source dataset | uspto-grants-2016_05 |
| ORD ID | ord-338e4b7ca7664907937d9fede6717129 |
| Source note | uspto-grants-2016_05 |