HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chloro-3-methylbenzene-1-sulfonyl chloride → 4-chloro-N-[5-chloro-2-(methylthio)phenyl]-3-methylbenzenesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chloro-3-methylbenzene-1-sulfonyl chloride | HCID 221001 | — |
| Reactant | 5-Chloro-2-(methylthio)aniline | HCID 2794577 | — |
| Product | 4-chloro-N-[5-chloro-2-(methylthio)phenyl]-3-methylbenzenesulfonamide | HCID 57378644 | 59.6% |
Reaction Steps
Following General Procedure B, the title compound (205 mg, 59%) was prepared from 5-chloro-2-methylsulfanyl-phenylamine (165 mg, 0.95 mmol) and 4-chloro-3-methyl-benzenesulfonyl chloride (215 mg, 0.95 mmol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09328067B2 |
| Source dataset | uspto-grants-2016_05 |
| ORD ID | ord-c1a8be0fa57c4bd8a9071dce5dd17d78 |
| Source note | uspto-grants-2016_05 |