HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyrazole-4-carboxylic acid → N-[4-(4-Piperidinomethyl-2-pyridyloxy)butyl]-pyrazole-4-carboxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyrazole-4-carboxylic acid | HCID 3015937 | — |
| Reactant | 4-(4-Piperidinomethyl-2-pyridyloxy)butylamine | HCID 15053125 | — |
| Product | N-[4-(4-Piperidinomethyl-2-pyridyloxy)butyl]-pyrazole-4-carboxamide | HCID 19962909 | 71% |
Reaction Steps
Following a procedure similar to that described in Example 64, but using 4-(4-piperidinomethyl-2-pyridyloxy)butylamine and 4-pyrazolecarboxylic acid as starting materials, in relative proportions similar to those used in that Example, the title compound was obtained as a white powder, melting at 145°-147° C., in a 71% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05616579 |
| Source dataset | uspto-grants-1997_04 |
| ORD ID | ord-98eb07bd13c94412bddb4d64150b7cfd |
| Source note | uspto-grants-1997_04 |