HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Bromide → 2-(Benzylthio)-5-chloroaniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Bromide | HCID 7498 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 2-Amino-4-chlorobenzenethiol | HCID 12000 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | 2-(Benzylthio)-5-chloroaniline | HCID 12618210 | 33.1% |
Reaction Steps
Following General Procedure A, the title compound (560 mg, 33%) was prepared from 2-amino-4-chlorobenzenethiol (1.08 g, 6.77 mmol), (bromomethyl)benzene (0.8 ml, 6.77 mmol) and K2CO3 (3.18 g, 23.04 mmol) in DMF (20 ml).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09328067B2 |
| Source dataset | uspto-grants-2016_05 |
| ORD ID | ord-d053fd71c89e4b1f82949bc852ffa452 |
| Source note | uspto-grants-2016_05 |