HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → Methyl 4-(((2-amino-4-chlorophenyl)thio)methyl)benzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 2-Amino-4-chlorobenzenethiol | HCID 12000 | — |
| Reactant | Methyl 4-(bromomethyl)benzoate | HCID 256687 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | Methyl 4-(((2-amino-4-chlorophenyl)thio)methyl)benzoate | HCID 28942620 | 88% |
Reaction Steps
Following General Procedure A, the title compound (2.2 g, 88%) was prepared from 2-amino-4-chlorobenzenethiol (1.3 g, 8.14 mmol), methyl 4-(bromomethyl)benzoate (1.86 g, 8.14 mmol) and K2CO3 (5.6 g, 40.73 mmol) in DMF (20 ml).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09328067B2 |
| Source dataset | uspto-grants-2016_05 |
| ORD ID | ord-6c4689c3ba4341fc9e6494c0b07762c4 |
| Source note | uspto-grants-2016_05 |