HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → 3-((2-amino-4-chlorophenyl)thio)-N,N-diethylpropanamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 2-Amino-4-chlorobenzenethiol | HCID 12000 | — |
| Reactant | 3-Bromo-n,n-diethylpropanamide | HCID 226112 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | 3-((2-amino-4-chlorophenyl)thio)-N,N-diethylpropanamide | HCID 86690994 | 88% |
Reaction Steps
Following General Procedure A, the title compound (1.0 g, 88%) was prepared from 2-amino-4-chlorobenzenethiol (660 mg, 4.13 mmol), crude 3-bromo-N,N-diethylpropanamide (860 mg, 6.60 mmol) and K2CO3 (2.9 g, 20.67 mmol) in DMF (20 ml).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09328067B2 |
| Source dataset | uspto-grants-2016_05 |
| ORD ID | ord-f5bc7b32479543f899791f54faab608d |
| Source note | uspto-grants-2016_05 |