HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Aminothiophenol → Methyl 2-(((2-aminophenyl)thio)methyl)benzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Aminothiophenol | HCID 8713 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Methyl 2-(bromomethyl)benzoate | HCID 2734813 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | Methyl 2-(((2-aminophenyl)thio)methyl)benzoate | HCID 82976125 | 74% |
Reaction Steps
Following General Procedure A, the title compound (1.7 g, 74%) was prepared from 2-aminobenzenethiol (1.1 g, 8.47 mmol), methyl 2-(bromomethyl)benzoate (1.9 g, 8.47 mmol), and K2CO3 (3.5 g, 25.4 mmol) in DMF (50 ml).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09328067B2 |
| Source dataset | uspto-grants-2016_05 |
| ORD ID | ord-067d6b8dbc7c4efbbdb5757d17c176d7 |
| Source note | uspto-grants-2016_05 |