HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Propargylamine → 10-Bromo-5,6-dihydro-benzo[f]quinoline
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Propargylamine | HCID 239041 | — |
| Edukt | 8-Bromo-1,2,3,4-tetrahydronaphthalen-2-one | HCID 4136187 | — |
| Produkt | 10-Bromo-5,6-dihydro-benzo[f]quinoline | HCID 58294583 | 49% |
Reaktionsschritte
The title compound is prepared from 8-bromo-2-tetralone and propargylamine following a procedure analogous to that described in Step 1 of Intermediates 1 and 2. Yield: 49% of theory; LC (method 1): tR=2.68 min; Mass spectrum (ESI+): m/z=260/262 (Br) [M+H]+.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US09328072B2 |
| Quelldatensatz | uspto-grants-2016_05 |
| ORD ID | ord-884bce44ee47446b9416ef45e62e1b84 |
| Quellennotiz | uspto-grants-2016_05 |