HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylboronic Acid → HCID 58294596, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylboronic Acid | HCID 66827 | — |
| Reactant | trifluoro-methanesulfonic acid cis-1-(2,2,2-trifluoro-acetyl)-2,3,4,4a,9,9a-hexahydro-1H-indeno[2,1-b]pyridin-6-yl ester | HCID 58294405 | — |
| Product | HCID 58294596 | HCID 58294596 | 70% |
Reaction Steps
The title compound is prepared from trifluoro-methanesulfonic acid cis-1-(2,2,2-trifluoro-acetyl)-2,3,4,4a,9,9a-hexahydro-1H-indeno[2,1-b]pyridin-6-yl ester and phenylboronic acid following a procedure analogous to that described in Step 2 of Intermediates 17 and 18. Yield: 70% of theory; LC (method 1): tR=5.02 min; Mass spectrum (ESI+): m/z=346 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09328072B2 |
| Source dataset | uspto-grants-2016_05 |
| ORD ID | ord-5a97dc5f214342c6b0bbf39350d5af8e |
| Source note | uspto-grants-2016_05 |