HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 21969206, compound → (1H-Benzoimidazol-5-yl)-(trans-8-methoxy-2,3,4a,5,6,10b-hexahydro-1H-benzo[f]quinolin-4-yl)-methanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 21969206 | HCID 21969206 | — |
| Reactant | HCID 178524171 | HCID 178524171 | — |
| Product | (1H-Benzoimidazol-5-yl)-(trans-8-methoxy-2,3,4a,5,6,10b-hexahydro-1H-benzo[f]quinolin-4-yl)-methanone | HCID 178487173 | 71% |
Reaction Steps
The title compound is prepared from 1H-benzoimidazole-5-carboxylic acid and trans-8-methoxy-1,2,3,4,4a,5,6,10b-octahydro-benzo[f]quinoline following a procedure analogous to that described in Example 1. Yield: 71% of theory; LC (method 1): tR=2.61 min; Mass spectrum (ESI+): m/z=362 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09328072B2 |
| Source dataset | uspto-grants-2016_05 |
| ORD ID | ord-e26f0f5c4e984c36aa52b6b2c016b355 |
| Source note | uspto-grants-2016_05 |