HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → HCID 178485262, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | HCID 178524091 | HCID 178524091 | — |
| Product | HCID 178485262 | HCID 178485262 | 75% |
Reaction Steps
The title compound is prepared from cis-4-(1H-benzoimidazole-5-carbonyl)-1,2,3,4,4a,5,6,10b-octahydro-benzo[f]quinoline-8-carboxylic acid and methylamine (2 mol/L in tetrahydrofuran) following a procedure analogous to that described in Example 1. Yield: 75% of theory; LC (method 1): tR=1.91 min; Mass spectrum (ESI+): m/z=389 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09328072B2 |
| Source dataset | uspto-grants-2016_05 |
| ORD ID | ord-f5bcaa814ca245ad8d6ac99636972935 |
| Source note | uspto-grants-2016_05 |