HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86611633, compound → HCID 69507055, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86611633 | HCID 86611633 | — |
| Reactant | HCID 178418255 | HCID 178418255 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 69507055 | HCID 69507055 | — |
Reaction Steps
The general method described in Step 6 of Example 15 was used to react N-methoxy-N-methyl-12-(2-propyl-1H-imidazo[4,5-c]quinolin-1-yl)dodecanamide (6.0 g, 13.3 mmol) with phenylmagnesium bromide (26.5 mmol, 26.5 mL of a 1 M solution in THF) to provide 1-phenyl-12-(2-propyl-1H-imidazo[4,5-c]quinolin-1-yl)dodecan-1-one (6.0 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09328110B2 |
| Source dataset | uspto-grants-2016_05 |
| ORD ID | ord-ff09e234ee884addaa67c5b0dd427981 |
| Source note | uspto-grants-2016_05 |