HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 68876533, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 2,2-Diethoxyethylamine | HCID 69524 | — |
| Reactant | 4-Chloro-3-nitroquinoline | HCID 11275808 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 68876533 | HCID 68876533 | 97.3% |
Reaction Steps
The general method described in Step 1 of Example 1 was used to react 4-chloro-3-nitroquinoline (20.9 g, 100 mmol), aminoacetaldehyde diethyl acetal (14.4 g, 110 mmol), and triethylamine (12.6 g, 125 mmol) in dichloromethane for 15 hours to provide (2,2-diethoxyethyl)-(3-nitroquinolin-4-yl)amine (29.7 g) as a yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09328110B2 |
| Source dataset | uspto-grants-2016_05 |
| ORD ID | ord-ebb125db7b4e45b381d8a18be44affad |
| Source note | uspto-grants-2016_05 |