HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 57455410, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 1-Amino-3,3-diethoxypropane | HCID 521029 | — |
| Reactant | 4-Chloro-3-nitroquinoline | HCID 11275808 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 57455410 | HCID 57455410 | 98.4% |
Reaction Steps
The general method described in Step 1 of Example 1 was used to react 4-chloro-3-nitroquinoline (20.3 g, 97.1 mmol), 1-amino-3,3-diethoxypropane (25.0 g, 116 mmol) and triethylamine (33.8 g, 333 mmol) in dichloromethane for 15 hours to provide (3,3-diethoxypropyl)-(3-nitroquinolin-4-yl)amine (30.5 g) as a yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09328110B2 |
| Source dataset | uspto-grants-2016_05 |
| ORD ID | ord-a256694c56b042e5a5b73a2ccbae8296 |
| Source note | uspto-grants-2016_05 |