HCID 89656278, compound → HCID 89656024, compound

Participants

Reaction Steps

A mixture of methyl 4-bromo-9-oxo-5,6,7,8,9,10-hexahydroacridine-1-carboxylate (0.19 g, 0.56 mmol), MeOH (20 mL), and Pd/C (5% Pd on carbon, 50% water, 0.05 g) were stirred at room temperature under an atmosphere of hydrogen for 6 hours. The mixture was filtered through celite and the filtrate was concentrated to give crude methyl 9-oxo-5,6,7,8,9,10-hexahydroacridine-1-carboxylate (0.22 g), which was used to next step without further purification.

Provenance & Evidence