HCID 131735502, compound → HCID 90111508, compound

Participants

Reaction Steps

A solution of 2-(diallylamino)-1-(3-pyridyl)ethanone oxime (3.95 g, 17.08 mmol) in toluene (56 mL) is heated at 120° C. for 18 hours. The solvent is removed under reduced pressure. The crude product is purified by silica gel column chromatography using a 0-5% gradient of 0.14 M ammonia/methanol solution in dichloromethane to give the title compound (2.14 g, 43%). ES/MS (m/e): 232 (M+1).

Provenance & Evidence