HRID522107

反应详情

EQUATION

反应方程式

HRID 522107 的结构方程式

PROCEDURE

实验过程

The title compound was prepared according to the method described for Example 99 using 2-chloro-4-methoxy-5-(pyridin-2-yl)benzoic acid (Preparation 26) and 5-amino-1-phenyl-1H-pyrazole-3-carbonitrile (Preparation 53). The residue was purified using reverse phase chromatography eluting with 5-60% MeCN (with 0.1% formic acid) in water (with 0.1% formic acid).

WORKUP

后处理

  1. customThe residue was purified
  2. washeluting with 5-60% MeCN (with 0.1% formic acid) in water (with 0.1% formic acid)