HuagongsheHuagongshe Chemistry Print Report · For research reference only
Heptanoic Acid → 2-Propylheptanoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Heptanoic Acid | HCID 8094 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 2-Propylheptanal | HCID 3018634 | — |
| Solvent | Water | HCID 962 | — |
| Product | 2-Propylheptanoic acid | HCID 35728 | — |
Reaction Steps
A reactor was charged with 0.2 g (0.005 mol) of sodium hydroxide (manufactured by Kanto Chemical Co., Inc.), 1 g of water, and 0.8 g (0.006 mol) of heptanoic acid (manufactured by Kishida Chemical Co., Ltd.), and the mixture was stirred. After the addition of 47 g of 2-propylheptanal, the mixture was bubbled with air at 40° C. for 15 hours. The mixture was stirred at 130° C. for 4 hours with nitrogen bubbling to obtain crude 2-propylheptanoic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09328306B2 |
| Source dataset | uspto-grants-2016_05 |
| ORD ID | ord-60a94c02c1db45ad99ce7e0235de28e4 |
| Source note | uspto-grants-2016_05 |