Acetic Acid → HCID 89590858, compound

Participants

Reaction Steps

To a solution of the product from Step 2 (34 mg, 0.060 mmol) in CH2Cl2 (3 ml) was added morpholine (0.016 ml, 0.180 mmol) and acetic acid (10.32 μl, 0.180 mmol) followed by sodium triacetoxyborohydride (38.2 mg, 0.180 mmol). The reaction was complete in 30 minutes at which stage it was quenched with water and extracted with dichloromethane. Purification by PTLC (40% EtOAc/hexane) provided the desired compound.

Provenance & Evidence