HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → S 20928
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Cyclobutanecarbonyl chloride | HCID 78705 | — |
| Reactant | 2-(1-Naphthyl)ethylamine hydrochloride | HCID 12370437 | — |
| Solvent | Chloroform water | HCID 22418719 | — |
| Product | S 20928 | HCID 127856 | — |
Reaction Steps
0.01 mol of N-[2-(1-naphthyl)ethyl]amine hydrochloride is dissolved in a water/chloroform (40: 60; vol/vol ) mixture, and 0.02 mol of potassium carbonate is then added with magnetic stirring. The reaction mixture is cooled in an ice bath, and 0.01 mol of cyclobutanecarbonyl chloride is then added dropwise with magnetic stirring.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05616614 |
| Source dataset | uspto-grants-1997_04 |
| ORD ID | ord-8e4b4b7fd8854a2684e0c0c78407b175 |
| Source note | uspto-grants-1997_04 |