2-Methoxyethylamine → 2-(Dimethylamino)ethylamino-5-(2-methoxy ethylamino)anthracene-9,10-dione

HRID 522939노트

반응식

HRID 522939 반응식
Cl[C:2]1[C:15]2[C:14](=[O:16])[C:13]3[C:8](=[C:9]([NH:17][CH2:18][CH2:19][N:20]([CH3:22])[CH3:21])[CH:10]=[CH:11][CH:12]=3)[C:7](=[O:23])[C:6]=2[CH:5]=[CH:4][CH:3]=1.[CH3:24][O:25][CH2:26][CH2:27][NH2:28]>>[CH3:21][N:20]([CH3:22])[CH2:19][CH2:18][NH:17][C:9]1[C:8]2[C:7](=[O:23])[C:6]3[C:15](=[C:2]([NH:28][CH2:27][CH2:26][O:25][CH3:24])[CH:3]=[CH:4][CH:5]=3)[C:14](=[O:16])[C:13]=2[CH:12]=[CH:11][CH:10]=1

참가 물질

3

반응물 2

HCID 80182-MethoxyethylamineHCID 143201251-Chloro-5-(2-(dimethylamino)ethylamino)anthracene-9,10-dione

생성물 1

HCID 592291202-(Dimethylamino)ethylamino-5-(2-methoxy ethylamino)anthracene-9,10-dione

실험 절차

This procedure was carried out as described previously in step (a) of Example 15, using Compound 17 (0.25 g, 0.76 mmol) and 2-methoxyethylamin (0.66 mL, 7.6 mmol). This product was used in the next step without any purification. The structure of Compound 23 is given below:

후처리

  1. customThis product was used in the next step without any purification

출처 및 근거

ORD 기록
ord-286cfd9d7b2e4401a5c3495b392676e9
출처 데이터셋
uspto-grants-2016_05
특허 번호
US09334281B2

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