2-Methyl-2-butene → HCID 118676292, compound

Participants

Reaction Steps

To 50 mg (0.16 mmol) of 43 in each of t-BuOH H2O is added 0.84 mL (7.9 mmol) of 2-methyl-but-2-ene, 71 mg (0.79 mmol) of NaClO2 and 76 mg (0.63 mmol) of NaH2PO4. The mixture stirred for 1 h, and then 20 mL of saturated NH4Cl is added. The mixture is extracted three times with 20 mL of EtOAc, and the extract is dried with MgSO4, filtered, and concentrated to provide 46 mg (0.14 mmol) of 44.

Provenance & Evidence