Dithiooxamide → 2,5-Bis(3-tetradecoxycarbonyl-2-thienyl)-thiazolo[5,4-d]thiazole

Participants

Reaction Conditions

Reaction Steps

To a 25 mL flask were added 0.978 g (2.8 mmol) of tetradecyl-2-formylthiophene-3-carboxylate and 110 mg (0.9 mmol) of dithiooxamide. This mixture was heated to 200° C. for 2 hours. The resulting mixture was purified by column chromatography using a mixture of hexane and dichloromethane to give the desired compound. The NMR data were obtained and were consistent with those of the desired compound.

Provenance & Evidence