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HRID524135

反应详情

EQUATION

反应方程式

HRID 524135 的结构方程式

REACTANTS

反应物

2
结构：COC(=O)c1ccccc1S(=O)(=O)Cl
HCID117830

Benzoic acid, 2-(chlorosulfonyl)-, methyl ester

C8H7ClO4S

结构：COc1ccc(C2=NN(C3CCNCC3)C(=O)C2(C)C)cc1OC.Cl
HCID66616406

未命名化合物

2 次

PRODUCTS

生成物

1
结构：COC(=O)c1ccccc1S(=O)(=O)N1CCC(N2N=C(c3ccc(OC)c(OC)c3)C(C)(C)C2=O)CC1
HCID46189879

未命名化合物

PROCEDURE

实验过程

The title compound is prepared analogously as described for GP1 using 5-(3,4-dimethoxyphenyl)-4,4-dimethyl-2-(piperidin-4-yl)-2,4-dihydro-3H-pyrazol-3-one hydrochloride (compound B1*HCl) and methyl 2-(chlorosulfonyl)benzoate as starting compounds. The crude product is purified by crystallization from EA and diethyl ether to yield the title compound.

WORKUP

后处理

  1. customThe title compound is prepared analogously
  2. customThe crude product is purified by crystallization from EA and diethyl ether