HRID524155

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID76187

Benzenesulfonyl chloride, 2-chloro-

C6H4Cl2O2S

结构：COc1ccc(C2=NN(C3CCNCC3)C(=O)C2(C)C)cc1OC.Cl

HCID66616406

未命名化合物

2 次

PRODUCTS

生成物

结构：COc1ccc(C2=NN(C3CCN(S(=O)(=O)c4ccccc4Cl)CC3)C(=O)C2(C)C)cc1OC

HCID46203367

未命名化合物

PROCEDURE

实验过程

The title compound is prepared analogously as described for GP1 using 5-(3,4-dimethoxyphenyl)-4,4-dimethyl-2-(piperidin-4-yl)-2,4-dihydro-3H-pyrazol-3-one hydrochloride (compound B1*HCl) and 2-chlorobenzenesulfonyl chloride as starting compounds. The crude product is purified by crystallization from methanol to yield the title compound.

WORKUP

后处理

customThe title compound is prepared analogously
customThe crude product is purified by crystallization from methanol