HRID524206

反应详情

EQUATION

反应方程式

HRID 524206 的结构方程式

PROCEDURE

实验过程

The title compound is prepared analogously as described for GP3 using 5-(3,4-dimethoxyphenyl)-4,4-dimethyl-2-(piperidin-4-yl)-2,4-dihydro-3H-pyrazol-3-one (compound B1) and 4-amino-3-(trifluoromethyl)benzoic acid as starting compounds. The crude product is purified by column chromatography (silica gel and DCM/methanol=4:1) and crystallization from methanol to yield the title compound.

WORKUP

后处理

  1. customThe title compound is prepared analogously
  2. customThe crude product is purified by column chromatography (silica gel and DCM/methanol=4:1) and crystallization from methanol