HRID524222

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID79668

2-Acetoxybenzoyl chloride

C9H7ClO3

结构：COc1ccc(C2=NN(C3CCNCC3)C(=O)C2(C)C)cc1OC.Cl

HCID66616406

未命名化合物

2 次

PRODUCTS

生成物

结构：COc1ccc(C2=NN(C3CCN(C(=O)c4ccccc4OC(C)=O)CC3)C(=O)C2(C)C)cc1OC

HCID46202726

未命名化合物

PROCEDURE

实验过程

The title compound is prepared analogously as described for GP1 using 5-(3,4-dimethoxyphenyl)-4,4-dimethyl-2-(piperidin-4-yl)-2,4-dihydro-3H-pyrazol-3-one hydrochloride (compound B1*HCl) and 2-(chlorocarbonyl)phenyl acetate as starting compounds. The crude product is purified by crystallization from EA and diethyl ether to yield the title compound.

WORKUP

后处理

customThe title compound is prepared analogously
customThe crude product is purified by crystallization from EA and diethyl ether