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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 524231Generated: October 30, 2026

2,3-Dichlorobenzene-1-sulfonyl chloride → HCID 67365561, compound

https://huagongshe.com/reaction/524231

Reaction equation

Participants

RoleNameHCIDCharge
Reactant2,3-Dichlorobenzene-1-sulfonyl chlorideHCID 2734222—
Reactant5-(3,4-dimethoxyphenyl)-4,4-dimethyl-2-piperidin-4-yl-2,4-dihydro-3H-pyrazol-3-one hydrochlorideHCID 66616406—
ProductHCID 67365561HCID 67365561—

Reaction Steps

The title compound is prepared analogously as described for GP1 using 5-(3,4-dimethoxyphenyl)-4,4-dimethyl-2-(piperidin-4-yl)-2,4-dihydro-3H-pyrazol-3-one (compound B1) and 2,3-dichlorobenzenesulfonyl chloride as starting compounds. The crude product is purified by crystallization from EA and diethyl ether to yield the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09340522B2
Source datasetuspto-grants-2016_05
ORD IDord-1f0e3bfe7473472aa6ece9bdea2ae6c5
Source noteuspto-grants-2016_05