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HRID524335

反应详情

EQUATION

反应方程式

HRID 524335 的结构方程式

REACTANTS

反应物

5
结构：BrBr
HCID24408

Bromine

Br2

结构：CS(=O)(=O)c1ccc(CN)cc1.Cl
HCID2729269

1-[4-(Methanesulfonyl)phenyl]methanamine--hydrogen chloride (1/1)

C8H12ClNO2S

结构：CS(=O)(=O)c1ccc(CN)nc1
HCID57354332

1-[5-(Methanesulfonyl)pyridin-2-yl]methanamine

C7H10N2O2S

结构：Cc1c(Br)c(=O)c(C(=O)O)cn1C(C)C
HCID86711577

未命名化合物

结构：CC[C@H](C)n1cc(C(=O)O)c(=O)c(Br)c1C
HCID86711586

未命名化合物

PRODUCTS

生成物

1
结构：CC[C@H](C)n1cc(C(=O)NCc2ccc(S(C)(=O)=O)cn2)c(=O)c(Br)c1C
HCID86711585

未命名化合物

PROCEDURE

实验过程

Preparation 20 is prepared following the procedure for preparation 5, substituting preparation 3c with preparation 12b and 4-methylsulfonylbenzylamine hydrochloride with C-(5-methanesulfonyl-pyridin-2-yl)-methylamine. ESI mass spectrum: [M+H]+=456 (bromine isotope pattern); Retention time HPLC: 0.87 min (Z018_S04).

WORKUP

后处理

  1. customPreparation 20
  2. customis prepared
  3. customfor preparation 5
  4. custom0.87 min (Z018_S04)