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HRID524336

反应详情

EQUATION

反应方程式

HRID 524336 的结构方程式

REACTANTS

反应物

6
结构：CS(=O)(=O)c1ccc(CN)cc1.Cl
HCID2729269

1-[4-(Methanesulfonyl)phenyl]methanamine--hydrogen chloride (1/1)

C8H12ClNO2S

结构：CN(C)C(On1nnc2ccccc21)=[N+](C)C.F[P-](F)(F)(F)(F)F
HCID2733084

Methanaminium, N-[(1H-benzotriazol-1-yloxy)(dimethylamino)methylene]-N-methyl-, hexafluorophosphate(1-) (1:1)

C11H16F6N5OP

结构：CN(C)C(On1nnc2ccccc21)=[N+](C)C.F[B-](F)(F)F
HCID2733207

O-(Benzotriazol-1-yl)-N,N,N′,N′-tetramethyluronium tetrafluoroborate

C11H16BF4N5O

结构：CS(=O)(=O)c1ccc(CN)nc1
HCID57354332

1-[5-(Methanesulfonyl)pyridin-2-yl]methanamine

C7H10N2O2S

结构：Cc1c(Br)c(=O)c(C(=O)O)cn1C(C)C
HCID86711577

未命名化合物

结构：COCCn1cc(C(=O)O)c(=O)c(I)c1C
HCID86711579

未命名化合物

PRODUCTS

生成物

1
结构：COCCn1cc(C(=O)NCc2ccc(S(C)(=O)=O)cn2)c(=O)c(I)c1C
HCID86711587

未命名化合物

PROCEDURE

实验过程

Preparation 22 is prepared following the procedure for preparation 5, substituting preparation 3c with preparation 13b, 4-methylsulfonylbenzylamine hydrochloride with C-(5-methanesulfonyl-pyridin-2-yl)-methylamine and HBTU with TBTU. ESI mass spectrum: [M+H]+=506; Retention time HPLC: 0.90 min (Z003_003).

WORKUP

后处理

  1. customPreparation 22
  2. customis prepared
  3. customfor preparation 5