huagongshe.com
HRID524337

反应详情

EQUATION

反应方程式

HRID 524337 的结构方程式

REACTANTS

反应物

5
结构：BrBr
HCID24408

Bromine

Br2

结构：CS(=O)(=O)c1ccc(CN)cc1.Cl
HCID2729269

1-[4-(Methanesulfonyl)phenyl]methanamine--hydrogen chloride (1/1)

C8H12ClNO2S

结构：CS(=O)(=O)c1ccc(CN)nc1
HCID57354332

1-[5-(Methanesulfonyl)pyridin-2-yl]methanamine

C7H10N2O2S

结构：Cc1c(Br)c(=O)c(C(=O)O)cn1C(C)C
HCID86711577

未命名化合物

结构：Cc1c(Br)c(=O)c(C(=O)O)cn1C1CCOC1
HCID86711589

未命名化合物

PRODUCTS

生成物

1
结构：Cc1c(Br)c(=O)c(C(=O)NCc2ccc(S(C)(=O)=O)cn2)cn1C1CCOC1
HCID86711588

未命名化合物

PROCEDURE

实验过程

Preparation 22 is prepared following the procedure for preparation 5, substituting preparation 3c with preparation 14b and 4-methylsulfonylbenzylamine hydrochloride with C-(5-methanesulfonyl-pyridin-2-yl)-methylamine. ESI mass spectrum: [M+H]+=470 (bromine isotope pattern); Retention time HPLC: 0.77 min (Z018_S04).

WORKUP

后处理

  1. customPreparation 22
  2. customis prepared
  3. customfor preparation 5
  4. custom0.77 min (Z018_S04)