HCID 68182744, compound → HCID 68182616, compound

Participants

Reaction Steps

To a solution of tert-butyl 3-[(6-nitro-3-pyridyl)oxy]benzoate (1.0 g, 3.161 mmol), in ethyl acetate (20 mL) was added 10% Pd on carbon (0.2 g, 20% w/w), and reaction mixture was stirred under H2 gas balloon for 6 h. Completion of reaction was confirmed by TLC. Reaction mixture was filtered through celite pad washed with ethyl acetate, filtrate was concentrated under reduced pressure to afford pure product (0.9 g).

Provenance & Evidence