p-Chlorothiophenol → 2-Chloro-6-(4-chloro-phenylsulfanyl)-9-methyl-9H-purine

HRID 524498Notes

Reaction equation

HRID 524498 reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([SH:8])=[CH:4][CH:3]=1.[Cl:9][C:10]1[N:18]=[C:17]2[C:13]([N:14]=[CH:15][N:16]2[CH2:19]C)=[C:12](Cl)[N:11]=1>>[Cl:9][C:10]1[N:18]=[C:17]2[C:13]([N:14]=[CH:15][N:16]2[CH3:19])=[C:12]([S:8][C:5]2[CH:6]=[CH:7][C:2]([Cl:1])=[CH:3][CH:4]=2)[N:11]=1

Participants

3

Reactant 2

HCID 7815p-ChlorothiophenolHCID 219883252,6-dichloro-9-ethyl-9H-purine

Product 1

HCID 593222652-Chloro-6-(4-chloro-phenylsulfanyl)-9-methyl-9H-purine

Procedure

Was prepared according to Example 3 from 4-chlorobenzenethiol and 2,6-dichloro-9-ethyl-9H-purine.

Workup

  1. customWas prepared

Sources & evidence

ORD record
ord-1adc538e95c743308acc76d09b58ff59
Source dataset
uspto-grants-2016_05
Patent number
US09340544B2

Reaction notes

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