3-Methyl-2,4-pentanedione → (4-Chloro-phenyl)-[9-methyl-2-(3,4,5-trimethyl-pyrazol-1-yl)-9H-purin-6-yl]-amine
Reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([NH:8][C:9]2[N:17]=[C:16]([NH:18][NH2:19])[N:15]=[C:14]3[C:10]=2[N:11]=[CH:12][N:13]3[CH3:20])=[CH:4][CH:3]=1.[CH3:21][CH:22]([C:26](=O)[CH3:27])[C:23](=O)[CH3:24]>>[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([NH:8][C:9]2[N:17]=[C:16]([N:18]3[C:26]([CH3:27])=[C:22]([CH3:21])[C:23]([CH3:24])=[N:19]3)[N:15]=[C:14]3[C:10]=2[N:11]=[CH:12][N:13]3[CH3:20])=[CH:4][CH:3]=1Participants
3
Procedure
Was prepared according to Example 9 from (4-chloro-phenyl)-(2-hydrazino-9-methyl-9H-purin-6-yl)-amine and 3-methyl-2,4-pentanedione.
Workup
- customWas prepared
Sources & evidence
- ORD record
- ord-a1e69d3276334dc99c0a39ae1f1eba84
- Source dataset
- uspto-grants-2016_05
- Patent number
- US09340544B2
Reaction notes
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