HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-bromobutanimide → HCID 118107517, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | HCID 118107604 | HCID 118107604 | — |
| Product | HCID 118107517 | HCID 118107517 | 57% |
Reaction Steps
Ethyl 4-(2,4-dichlorophenyl)-6-methyl-2-(thiazol-4-yl)-1,4-dihydropyrimidine-5-carboxylate (5.31 g, 13.4 mmol) (The compound was synthesized according to the procedure as described in CN200610098646.3) was reacted with NBS (2.87 g, 16.1 mmol) according to the procedure as described in Example 1, Step B to give the title compound as a yellow solid (3.63 g, 57%). The compound was characterized by the following spectroscopic data:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09340538B2 |
| Source dataset | uspto-grants-2016_05 |
| ORD ID | ord-509ff2e950cc4ef8b299c49a140bbfa0 |
| Source note | uspto-grants-2016_05 |