Ammonium Chloride → HCID 178479323, compound

HRID 524753Notes

Reaction equation

[NH:1]1[CH:5]=[N:4][C:3]([C:6]#[N:7])=[N:2]1.C[O-].[Na+].[Cl-:11].[NH4+:12]>>[ClH:11].[NH:1]1[CH:5]=[N:4][C:3]([C:6](=[NH:12])[NH2:7])=[N:2]1

Participants

Reactant 3

HCID 25517Ammonium Chloride

HCID 10942334Sodium Methoxide

HCID 178510603HCID 178510603, compound

Product 1

HCID 178479323HCID 178479323, compound

Procedure

1H-1,2,4-triazole-3-carbonitrile (0.94 g, 10 mmol) was reacted with sodium methoxide (0.81 g, 15 mmol) and ammonium chloride (0.96 g, 18 mmol) according to the procedure as described in Example 61, Step B to give the title compound as an offwhite solid (0.59 g, 40%). The compound was characterized by the following spectroscopic data:

Sources & evidence

ORD record: ord-e763f25dac2f4c6ebe47a50bde960e87
Source dataset: uspto-grants-2016_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US09340538B2

Reaction notes

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