HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl Acetoacetate → HCID 118107614, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl Acetoacetate | HCID 8868 | — |
| Reactant | 2-Bromo-4-fluorobenzaldehyde | HCID 2773319 | — |
| Reactant | HCID 90043393 | HCID 90043393 | — |
| Product | HCID 118107614 | HCID 118107614 | 45% |
Reaction Steps
5-fluorothiazole-2-carboximidamide acetate (0.22 g, 1.07 mmol) was reacted with 2-bromo-4-fluorobenzaldehyde (0.22 g, 1.07 mmol) and ethyl 3-oxobutanoate (0.14 g, 1.07 mmol) according to the procedure as described in Example 1, Step A to give the title compound as a yellow solid (0.21 g, 45%). The compound was characterized by the following spectroscopic data:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09340538B2 |
| Source dataset | uspto-grants-2016_05 |
| ORD ID | ord-a591a408a7954508bd5c177a541fcc8f |
| Source note | uspto-grants-2016_05 |