HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-bromobutanimide → HCID 118107522, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | HCID 118107605 | HCID 118107605 | — |
| Product | HCID 118107522 | HCID 118107522 | 70% |
Reaction Steps
Ethyl 4-(2,4-dichlorophenyl)-2-(5-fluorothiazol-2-yl)-6-methyl-1,4-dihydropyrimidine-5-carboxylate (0.44 g, 1.06 mmol) was reacted with NBS (0.19 g, 1.06 mmol) according to the procedure as described in Example 1, Step B to give the title compound as a yellow solid (0.36 g, 70%). The compound was characterized by the following spectroscopic data:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09340538B2 |
| Source dataset | uspto-grants-2016_05 |
| ORD ID | ord-4b64808ac642487d85ab2ec9230d5bbe |
| Source note | uspto-grants-2016_05 |