HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Amino-6-methoxybenzothiazole → 2-Cyano-6-methoxy benzothiazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Amino-6-methoxybenzothiazole | HCID 15630 | — |
| Reactant | HCID 178418546 | HCID 178418546 | — |
| Product | 2-Cyano-6-methoxy benzothiazole | HCID 342109 | 22.1% |
Reaction Steps
6-methoxybenzo[d]thiazol-2-amine (9 g, 50 mmol) was reacted with CuCN (8.96 g, 100 mmol) according to the procedure as described in Example 61, Step A to give the title compound as a white solid (2.1 g, 22%). The compound was characterized by the following spectroscopic data:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09340538B2 |
| Source dataset | uspto-grants-2016_05 |
| ORD ID | ord-f2c31f5651ce4d4bbb0f55cdedf1b63b |
| Source note | uspto-grants-2016_05 |