HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chloroacetyl chloride → HCID 90042539, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chloroacetyl chloride | HCID 6577 | — |
| Reactant | HCID 90044060 | HCID 90044060 | — |
| Product | HCID 90042539 | HCID 90042539 | 65% |
Reaction Steps
(S)-2-(benzylamino)-3-hydroxy-2-methylpropanoic acid (2.09 g, 10 mmol) was reacted with chloroacetyl chloride (1.74 g, 15.4 mmol) according to the procedure as described in Example 46, Step B to give the title compound as a gray solid (1.62 g, 65%). The compound was characterized by the following spectroscopic data:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09340538B2 |
| Source dataset | uspto-grants-2016_05 |
| ORD ID | ord-c334f5bce7f64d43b5a2aa6e350c6e73 |
| Source note | uspto-grants-2016_05 |