HuagongsheHuagongshe Chemistry Print Report · For research reference only
Borane → HCID 118118263, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Borane | HCID 6331 | — |
| Reactant | HCID 118118264 | HCID 118118264 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 118118263 | HCID 118118263 | 70.7% |
Reaction Steps
(S)-benzyl 4-benzyl-3-methyl-5-oxomorpholine-3-carboxylate (3.4 g, 10 mmol) was reacted with a solution of borane in THF (1 mol/L, 20 mL) according to the procedure as described in Example 34, Step B to give the title compound as colorless oil (2.3 g, 70%). The compound was characterized by the following spectroscopic data:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09340538B2 |
| Source dataset | uspto-grants-2016_05 |
| ORD ID | ord-86a09b8585a44649afe2e82f5121e5f0 |
| Source note | uspto-grants-2016_05 |