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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 524832Generated: October 30, 2026

Borane → HCID 118118263, compound

https://huagongshe.com/reaction/524832

Reaction equation

Participants

RoleNameHCIDCharge
ReactantBoraneHCID 6331—
ReactantHCID 118118264HCID 118118264—
SolventTetrahydrofuranHCID 8028—
ProductHCID 118118263HCID 11811826370.7%

Reaction Steps

(S)-benzyl 4-benzyl-3-methyl-5-oxomorpholine-3-carboxylate (3.4 g, 10 mmol) was reacted with a solution of borane in THF (1 mol/L, 20 mL) according to the procedure as described in Example 34, Step B to give the title compound as colorless oil (2.3 g, 70%). The compound was characterized by the following spectroscopic data:

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09340538B2
Source datasetuspto-grants-2016_05
ORD IDord-86a09b8585a44649afe2e82f5121e5f0
Source noteuspto-grants-2016_05