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HRID525000

反应详情

EQUATION

反应方程式

HRID 525000 的结构方程式

REACTANTS

反应物

2
结构：C[C@H](NC(=O)OC(C)(C)C)C(=O)O
HCID85082

L-Alanine, N-[(1,1-dimethylethoxy)carbonyl]-

C8H15NO4

结构：Cc1ccn(N)c1C(=O)Nc1ccccc1
HCID70922439

未命名化合物

PRODUCTS

生成物

1
结构：Cc1ccn(NC(=O)[C@H](C)NC(=O)OC(C)(C)C)c1C(=O)Nc1ccccc1
HCID90200400

未命名化合物

收率 23%

PROCEDURE

实验过程

Prepared from 2.00 g (9.29 mmol) of 1-amino-3-methyl-N-phenyl-1H-pyrrole-2-carboxamide and 2.11 g (11.15 mmol) of (S)-2-(tert-butoxycarbonylamino)propanoic acid following the experimental procedure described in Preparation 22a. After purification by flash chromatography (0 to 10% methanol in dichloromethane), 825 mg (23% yield) of the title product were obtained.

WORKUP

后处理

  1. customAfter purification by flash chromatography (0 to 10% methanol in dichloromethane)