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HRID525029

反应详情

EQUATION

反应方程式

HRID 525029 的结构方程式

REACTANTS

反应物

2
结构：NCc1ccccc1Cl
HCID66648

2-Chlorobenzylamine

C7H8ClN

结构：COC(=O)c1c(Br)ccn1NC(=O)[C@H](C)NC(=O)OC(C)(C)C
HCID86722018

未命名化合物

PRODUCTS

生成物

1
结构：C[C@H](NC(=O)OC(C)(C)C)C(=O)Nn1ccc(Br)c1C(=O)NCc1ccccc1Cl
HCID86722048

未命名化合物

收率 65%

PROCEDURE

实验过程

The title compound was prepared from (S)-Methyl 3-bromo-1-(2-(tert-butoxycarbonylamino)propanamido)-1H-pyrrole-2-carboxylate (310 mg, 0.8 mmol) and (2-chlorophenyl)methanamine (385 μL, 3.2 mmol) following the experimental procedure described in Preparation 44a. 259 mg (65% yield) of the desired compound were obtained.