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HRID525677

反应详情

EQUATION

反应方程式

HRID 525677 的结构方程式

REACTANTS

反应物

2
结构：CCNCCO
HCID8072

2-(Ethylamino)ethanol

C4H11NO

结构：O=C(Nc1ccc(OC(F)(F)Cl)cc1)c1cnc(Cl)c(Br)c1
HCID72546089

未命名化合物

PRODUCTS

生成物

1
结构：CCN(CCO)c1ncc(C(=O)Nc2ccc(OC(F)(F)Cl)cc2)cc1Br
HCID89906841

未命名化合物

PROCEDURE

实验过程

The title compound was prepared in an analogous fashion to that described in Stage 22.1 using 5-bromo-6-chloro-N-(4-(chlorodifluoromethoxy)phenyl)nicotinamide (Stage 22.2) and 2-ethylamino-ethanol to afford an off-white crystalline solid. (Reaction Time was 10 h). HPLC (Condition 4) tR=6.1 min, UPLC-MS (Condition 3) tR=1.21 min, m/z=466.2 [M+H]+.

WORKUP

后处理

  1. customto afford an off-white crystalline solid
  2. custom(Reaction Time was 10 h)