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HRID 525755作成日：2026年10月25日

1,4-Dideoxy-1,4-iminothreitol → HCID 89906400、化合物

https://huagongshe.com/reaction/525755

反応式

関与物質

役割名称HCID仕込み量
反応物1,4-Dideoxy-1,4-iminothreitolHCID 146198—
反応物3-bromo-N-(4-(chlorodifluoromethoxy)phenyl)-4-fluorobenzamideHCID 86702622—
生成物HCID 89906400HCID 89906400—

反応手順

The title compound was prepared in an analogous fashion to that described in Example 1 using 3-bromo-N-(4-(chlorodifluoromethoxy)phenyl)-4-fluorobenzamide (Stage 76.2) and (3S,4S)-pyrrolidine-3,4-diol. The crude product was purified by flash chromatography (Silica gel column, 12 g, n-hexane/EtOAc 10% to 100% EtOAc) to give the title product as a white solid. UPLC-MS (Condition 8) tR=1.02 min, m/z=477.1/478.9 [M+H]+.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US09340537B2
出典データセットuspto-grants-2016_05
ORD IDord-31dc8ff6ceea40bebd7a10271bc864b2
出典メモuspto-grants-2016_05