(+-)-2-Butanol → Benzenepropanol, .alpha.-ethyl-.alpha.-methyl-

HRID 525783Notes

Reaction equation

HRID 525783 reaction equation
[CH2:1]=[CH:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1.[CH3:9][CH:10]([OH:13])[CH2:11][CH3:12]>>[CH3:9][C:10]([OH:13])([CH2:11][CH3:12])[CH2:1][CH2:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1

Participants

3

Reactant 2

HCID 6568(+-)-2-ButanolHCID 7501Styrene2×

Product 1

HCID 61516Benzenepropanol, .alpha.-ethyl-.alpha.-methyl-

Procedure

A solution of styrene in 2-butanol (20% by weight, 100 g/h) was pumped continuously at an average temperature of 390° C. in the reactor through the laboratory plant. The conversion of styrene was 84.0% and, in the steady state, 14.7 g/h of 3-methyl-1-phenyl-3-pentanol were obtained.

Workup

  1. customwas pumped continuously at an average temperature of 390° C. in the reactor through the laboratory plant

Sources & evidence

ORD record
ord-5e3fba91091d417589e43a2bf7bb276e
Source dataset
uspto-grants-2016_05
Patent number
US09340754B2

Reaction notes

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