HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 137231656, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 137231655 | HCID 137231655 | — |
| Product | HCID 137231656 | HCID 137231656 | 70% |
Reaction Steps
Prepared analogously to Example 5e) from (R)-N5 -[amino(nitroimino)methyl]-N2 -[(tert.-butyloxy)carbonyl]-N-[(4-ethoxyphenyl)methyl]-ornithinamide by the action of trifluoroacetic acid in a yield of 70% of theory. The base liberated from the salt by treatment with 1N sodium hydroxide solution melted at 182°-184° C. (ethyl acetate).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05616620 |
| Source dataset | uspto-grants-1997_04 |
| ORD ID | ord-0e47177b57e3422fa256272dff76bd63 |
| Source note | uspto-grants-1997_04 |