HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,8-Dichloro-7-(methylsulfonyl)-1,5-naphthyridine → HCID 178484104, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,8-Dichloro-7-(methylsulfonyl)-1,5-naphthyridine | HCID 117773033 | — |
| Reactant | HCID 178484109 | HCID 178484109 | — |
| Product | HCID 178484104 | HCID 178484104 | 34.2% |
Reaction Steps
Following general procedure I, 2,8-dichloro-7-(methylsulfonyl)-1,5-naphthyridine (140 mg, 0.52 mmol) was reacted with trans-N1,N1-dimethylcyclohexane-1,4-diamine dihydrochloride (140 mg, 0.65 mmol) to afford the desired product (68 mg, 34%) as an off-white solid: ESI MS m/z 383 [M+H]+
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09345709B2 |
| Source dataset | uspto-grants-2016_05 |
| ORD ID | ord-6cb901a9a5ee4139b6a331d81d4ec71a |
| Source note | uspto-grants-2016_05 |