HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(4,6-Dichloro-1,5-naphthyridin-3-yl)-2-oxoethyl acetate → HCID 178476434, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(4,6-Dichloro-1,5-naphthyridin-3-yl)-2-oxoethyl acetate | HCID 89705165 | — |
| Reactant | HCID 178483674 | HCID 178483674 | — |
| Product | HCID 178476434 | HCID 178476434 | 65.1% |
Reaction Steps
Following general procedure I, 2-(4,6-dichloro-1,5-naphthyridin-3-yl)-2-oxoethyl acetate (101 mg, 0.33 mmol) was reacted with trans-4-[(dimethylamino)methyl]cyclohexan amine (67 mg, 0.43 mmol) to afford the desired product (90 mg, 65%) as an off-white solid. ESI MS m/z 419 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09345709B2 |
| Source dataset | uspto-grants-2016_05 |
| ORD ID | ord-c8c1ed903af44c72a7ac2a66710fe6f7 |
| Source note | uspto-grants-2016_05 |