Hydroxylamine → HCID 71585544, compound

Participants

Reaction Steps

A solution of methyl 4-((2-methyl-1,2,3,4-tetrahydropyrimido[1,6-a]indol-5-yl)methyl)benzoate (0.07 g) and 1 mL of 50% aqueous solution of NH2OH in 3 mL of MeOH was stirred at r.t. for 12 h, and the reaction mixture was concentrated under vacuum. The residue was purified by silica gel chromatography eluted with up to 10% MeOH/CH2Cl2 to give 0.02 g of the title product as white solid.

Provenance & Evidence